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Cinnamamide
Other Names: Cinnamamide, predominantly trans; (Z)-3-phenylprop-2-enamide
CAS No: 621-79-4
EINECS No: 210-707-8
Formula: C9H9NO
Molar volume: 147.1739 (m3/mol）
Density: 1.121g/cm3
Melting point: 148-150 degrees Celsius(lit.)
Boiling Point: 350.3 degrees Celsius at 760 mmHg
Flash Point(degrees Celsius): 165.6 degrees Celsius
Appearance: White Crystal
Refractive Index (20 degrees Celsius): 1.613
Packing: 200kg/plastic Drum
- Landmark
- 621-79-4
Physical and chemical properties: white solid, slightly soluble in hot water, soluble in ethanol and ether.
Usage:
Used as an intermediate in organic synthesis.
Spices - mainly used for the preparation of gooseberry, peach, strawberry, cherry, cocoa and chocolate aroma strong flavor.
Storage:
Store in an airtight container and in a cool, dry place. Storage areas must be kept away from oxidants.
Synthesis method:
By chlorinating and acylation of cinnamic acid. Cinnamamide was distilled from the crude product by reduced pressure using cinnamic acid and dichlorosulfoxide at 60-70 degrees Celsius for 3-4 hours and the crude product was obtained by vacuum distillation. The cinnamoyl chloride was slowly added to the concentrated ammonia water below 30 degrees Celsius and stirred for 1 hour at the temperature below 30 degrees Celsius 24h, pour in a large amount of distilled water, centrifugally shake dry, wash, re-crystallize with dilute ethanol to get finished product.
Specifications
Item | REQUIREMENT | RESULT |
Assay | ≥98.5% | 99.42 % |
Description | White Crystal | White Crystal |
Melting point | 148-150 degrees Celsius | 148 degrees Celsius |
Refractive Index | 1.613 | 1.612 |
Flash point | 165.6 degrees Celsius | degrees Celsius |
Density | 1.121g/cm3 | 1.13g/cm3 |
Physical and chemical properties: white solid, slightly soluble in hot water, soluble in ethanol and ether.
Usage:
Used as an intermediate in organic synthesis.
Spices - mainly used for the preparation of gooseberry, peach, strawberry, cherry, cocoa and chocolate aroma strong flavor.
Storage:
Store in an airtight container and in a cool, dry place. Storage areas must be kept away from oxidants.
Synthesis method:
By chlorinating and acylation of cinnamic acid. Cinnamamide was distilled from the crude product by reduced pressure using cinnamic acid and dichlorosulfoxide at 60-70 degrees Celsius for 3-4 hours and the crude product was obtained by vacuum distillation. The cinnamoyl chloride was slowly added to the concentrated ammonia water below 30 degrees Celsius and stirred for 1 hour at the temperature below 30 degrees Celsius 24h, pour in a large amount of distilled water, centrifugally shake dry, wash, re-crystallize with dilute ethanol to get finished product.
Specifications
Item | REQUIREMENT | RESULT |
Assay | ≥98.5% | 99.42 % |
Description | White Crystal | White Crystal |
Melting point | 148-150 degrees Celsius | 148 degrees Celsius |
Refractive Index | 1.613 | 1.612 |
Flash point | 165.6 degrees Celsius | degrees Celsius |
Density | 1.121g/cm3 | 1.13g/cm3 |
